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| Registros recuperados : 11 | |
| 2. |  | PALLADINO, C.; PAREJA, L.; PEREYRA, S.; PÉREZ, C. Problems of pesticide residues in grains. [La problemática de los residuos de fitosanitarios en granos]. [Problemática dos resíduos de fitossanitários em grãos]. I Technical Conference of the Plant Protection Group - EEMAC. Agrociencia Uruguay, 2023, Vol.27 (Supplement), e1230. https://doi.org/10.31285/AGRO.27.1230 -- OPEN ACCESS. Article history: Received 24 Jul 2032; Accepted 25 Jul 2023; Published 11 Sep 2023. -- Editor: Horacio Silva, Universidad de la República, Facultad de Agronomía, Paysandú, Uruguay. -- Correspondence: Cintia Palladino,...| Biblioteca(s): INIA Las Brujas. |
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| 3. | | PALLADINO, C.; PÉREZ, C.A.; PAREJA, L.; PÉREZ-PARADA. A.; FRANCO, J.; PEREYRA, S. Fungicide strategies for Ramularia Leaf Spot control recommended in Uruguay and its residues in barley grains. [Estrategias de fungicidas recomendadas para el control de ramulariosis en Uruguay y sus residuos en granos de cebada.]. [Estratégias de fungicidas para o controlo da ramulariose recomendadas no Uruguai e respectivos resíduos nos grãos de cevada.]. Section. Plant protection. Agrociencia Uruguay, 2024, Vol.28, e1262. https://doi.org/10.31285/AGRO.28.1262 -- OPEN ACCESS. Article history: Received 04 October 2023; Accepted 01 December 2023; Published 01 February 2024. -- Editor: María Inés Siri, Universidad de la República, Montevideo, Uruguay. -- Correspondence: Cintia Palladino, cpalladino@cup.edu.uy --...| Biblioteca(s): INIA Las Brujas. |
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| 5. | | PALLADINO, C.; MUELA, A.; TABORDA, B.; PUIGVERT, F.; PÉREZ-PARADA, A.; COLAZZO, M.; PÉREZ, C. A.; PEREYRA, S.; PAREJA, L. Application of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain. ACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263 Article history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022.
Corresponding author: Pareja, L.; Departamento de Química Del...| Biblioteca(s): INIA Las Brujas. |
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| 6. | | PAREJA, L.; COLAZZO, M.; PÉREZ-PARADA, A.; NIELL, S.; CARRASCO-LETELIER, L.; BESIL, N.; CESIO, M.V.; HEINZEN, H. Detection of pesticides in active and depopulated beehives in Uruguay International Journal of Environmental Research and Public Health, 2011, v. 8, n. 10, p. 3844-3858 OPEN ACCESS ARTICLE.| Biblioteca(s): INIA La Estanzuela; INIA Las Brujas. |
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| 7. | | NIELL, S.; PAREJA, L.; ASTEGGIANTE, L.G.; ROEHRS, R.; PIZZUTTI, I.R.; GARCIA, C.; HEINZEN, H.; CESIO, M.V. Development of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition. Journal of AOAC International, 2010, v. 93 no.2, p. 425-431. 2-s2.0-77952781014| Biblioteca(s): INIA Las Brujas. |
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| 8. | | Cesio, V.; Pareja, L.; Niell, S.; Geis Asteggiante, L.; Bocking, B.; García, C.; Fernández, G.; Fernández-Alba, A.R.; Heinzen, H. Critical revision and development perspectives of herbicide residues analysis in Agro Ecosystems 1a.ed. ln: Kortekamp, A. (ed). Herbicides and environment. India: Intech, 2011. p.125-156| Biblioteca(s): INIA Las Brujas. |
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| 9. | | NIELL, S.; JESÚS, F.; PÉREZ, N.; PÉREZ, C.; PAREJA, L.; ABATTE, S.; CARRASCO-LETELIER, L.; DIAZ, S.; MENDOZA, Y.; CESIO, V.; HEINZEN, H. Neonicotinoids transference from the field to the hive by honey bees: Towards a pesticide residues biomonitor Science of the Total Environment, 2017, v. 581-582, p. 25-31 Article history: Received 3 October 2016 / Received in revised form 14 December 2016 / Accepted 2 January 2017 / Available online xxxx| Biblioteca(s): INIA La Estanzuela; INIA Las Brujas. |
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| 10. | | PÉREZ, A.; ALONSO, B.; ERNST, F.; RODRÍGUEZ, C.; CESIO, V.; HEINZEN, H.; COLAZZO, M.; PAREJA, L.; PEREIRA, A.; MÁRQUEZ, A.; ERRICO, E. Residuos de plaguicidas en compartimentos ambientales. Montevideo (UY): INIA, 2020. 30 p. (Serie FPTA-INIA; 90) Proyecto FPTA 324: "Estudio del impacto de las actuales prácticas agrícolas en los recursos hídricos del bajo Río Negro y Esteros de Farrapos.". Período de ejecución: Mayo 2014 - Junio 2017. Institución Ejecutora: Universidad de la...| Biblioteca(s): INIA Las Brujas. |
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| 11. | | PEREYRA, S.; CASTRO, M.; VERO, S.; SILVA, P.; CAL, A.; TISCORNIA, G.; GONZALEZ, N.; BENTOS, D.; ALVAREZ, W.; RABAZA, S.; SEVILLANO, L.; BRANCATTI, G.; FRANCIA, C.; RAFFO, M.A.; GERMAN, S.; PÉREZ, C.; GARMENDIA, G.; PAREJA, L.; RODRÍGUEZ, A.; PENDAS, C.; QUINCKE, M.; VÁZQUEZ, D.; RODRIGUEZ, M. Fusariosis de la espiga en trigo y micotoxinas asociadas: contribuyendo a reducir su riesgo. Cultivos. Revista INIA Uruguay, Diciembre 2023, no.75 p.54-58. (Revista INIA; 75).| Biblioteca(s): INIA Las Brujas. |
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| Registros recuperados : 11 | |
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 | Acceso al texto completo restringido a Biblioteca INIA Las Brujas. Por información adicional contacte bibliolb@inia.org.uy. |
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Registro completo
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Biblioteca (s) : |
INIA Las Brujas. |
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Fecha actual : |
17/05/2022 |
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Actualizado : |
17/05/2022 |
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Tipo de producción científica : |
Artículos en Revistas Indexadas Internacionales |
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Circulación / Nivel : |
Internacional - -- |
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Autor : |
PALLADINO, C.; MUELA, A.; TABORDA, B.; PUIGVERT, F.; PÉREZ-PARADA, A.; COLAZZO, M.; PÉREZ, C. A.; PEREYRA, S.; PAREJA, L. |
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Afiliación : |
CINTIA PALLADINO, PDU Abordaje Holístico Al Impacto de Los Agroquímicos, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; AGUSTINA MUELA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; BELÉN TABORDA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; FLORENCIA PUIGVERT, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; ANDRÉS PÉREZ-PARADA, Departamento de Desarrollo Tecnológico - DDT, Centro Universitario Regional Del Este, Universidad de la República, Ruta 9 y Ruta 15, 27000, Rocha, Uruguay; MARCOS COLAZZO, Licenciatura en Análisis Alimentario, Inst. Tecnologico Regional Suroeste, Universidad Tecnologica, Calle 17, Saladero Santa Maria, 60000, Paysandu, Uruguay; CARLOS A. PÉREZ, Departamento de Protección Vegetal, Facultad de Agronomía, Universidad de la República, EEMAC, Ruta 3 km 363, Paysandu, 60000, Uruguay; SILVIA ANTONIA PEREYRA CORREA, INIA (Instituto Nacional de Investigación Agropecuaria), Uruguay; LUCÍA PAREJA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay. |
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Título : |
Application of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain. |
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Fecha de publicación : |
2022 |
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Fuente / Imprenta : |
ACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263 |
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ISSN : |
2692-1952 |
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DOI : |
10.1021/acsagscitech.1c00263 |
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Idioma : |
Inglés |
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Notas : |
Article history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022.
Corresponding author: Pareja, L.; Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, Uruguay; email:lpareja@fq.edu.uy -- |
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Contenido : |
ABSTRACT. A multiclass methodology to determine deoxynivalenol, zearalenone, and 13 widely used fungicides to control the main diseases in barley and wheat crops was optimized and validated. Three QuEChERS methods were compared in terms of recovery and repeatability. The recoveries of the validated method were in the 67-128% range for the selected compounds and relative standard deviations were below 20% according to Document SANTE No. 12682/2019. The limits of quantification (LOQs) were between 10 and 100 μg kg-1. The method was applied for the analysis of barley and wheat grains obtained under production conditions. These samples contained mycotoxins and fungicide residues at concentrations below the LOQs, except for carbendazim in wheat, which exceeded the Codex maximum residue levels. The results of this study provide a fast and simple analytical tool to evaluate the primary production of these grains and to identify possible risks to human health.
© 2022 American Chemical Society. |
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Palabras claves : |
Cereals; Food safety; Fungicide residues; Hyphenated chromatographic techniques; Mycotoxins. |
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Thesagro : |
CEREALES. |
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Asunto categoría : |
F01 Cultivo |
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Marc : |
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245 $aApplication of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain.$h[electronic resource]
260 $c2022
500 $aArticle history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022. Corresponding author: Pareja, L.; Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, Uruguay; email:lpareja@fq.edu.uy --
520 $aABSTRACT. A multiclass methodology to determine deoxynivalenol, zearalenone, and 13 widely used fungicides to control the main diseases in barley and wheat crops was optimized and validated. Three QuEChERS methods were compared in terms of recovery and repeatability. The recoveries of the validated method were in the 67-128% range for the selected compounds and relative standard deviations were below 20% according to Document SANTE No. 12682/2019. The limits of quantification (LOQs) were between 10 and 100 μg kg-1. The method was applied for the analysis of barley and wheat grains obtained under production conditions. These samples contained mycotoxins and fungicide residues at concentrations below the LOQs, except for carbendazim in wheat, which exceeded the Codex maximum residue levels. The results of this study provide a fast and simple analytical tool to evaluate the primary production of these grains and to identify possible risks to human health. © 2022 American Chemical Society.
650 $aCEREALES
653 $aCereals
653 $aFood safety
653 $aFungicide residues
653 $aHyphenated chromatographic techniques
653 $aMycotoxins
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700 1 $aPUIGVERT, F.
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773 $tACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263
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